Overview
Empyrean is the only platform that does it all, delivering the best data quality on every sample types. It covers the largest set of X-ray diffraction, scattering and imaging applications in one single instrument. Moreover, Empyrean not only meets the high expectations of scientists and XRD experts today, but will continue to do so as research themes evolve Empyrean is ideal for teaching purposes, thanks to the large doors that open completely, allowing access to the system to several people; but at the same time is perfect to perform measurements in demanding R&D environments in several industries.
Features and benefits
Highest data quality on every sample
Praised by scientists for its performance, Empyrean allows them to prepare for synchrotron beam time in the best possible way. The unrivalled collection of sample stages and optical components for Empyrean allows applications to be done in various ways: from ‘simple’ by just adding a few slits and analysis software to a standard geometry, to top performance using dedicated optics, sources and detectors. This is ideal for a multipurpose laboratory: if the need for a certain application increases, data quality and throughput time can be improved by adding dedicated modules.
Multipurpose and future proof
“The only thing constant in life is change”. This holds especially in a research environment, where the analytical needs often change with a redirection of the research program. New applications are easily added to an Empyrean system, making it the perfect answer for anything the feature will hold. New and exciting applications are constantly developed on this platform, keeping our customers on the cutting edge of technology.
Hybrid PIXel technologies
Malvern Panalytical has always been at the forefront of hybrid detector technology. We were the first company to introduce combined 0D and 1D functionality in silicon strip detectors and to expand the onboard flexibility to 0D-1D-2D-3D. The small pixel size, zero background and the high dynamic range of our hybrid detectors (PIXcel3D and GaliPIX3D) bring with them a revolution in the way XRD applications are treated. No longer is it necessary to maximize intensity or 2D detector size. With a choice of optics and operational radii, you can optimize the configuration to really suit your purpose.
MultiCore Optics
The newly developed MultiCore Optics featuring the iCore and dCore, greatly simplify the usage of a multipurpose system, bringing automation to a level never been seen before. When switching between measurements the iCore and dCore take care of the work and do not need any human intervention.
PreFIX
PreFIX is our proven proprietary concept that stands for pre-aligned fast interchangeable X-ray modules.
Thanks to this PreFIX concept your diffraction system becomes flexible, fast and future proof. The PreFIX mounting method of optics and stages enables the diffractometer to be reconfigured thanks to a reproducible positioning in three dimensions with microns precision. This allows users to switch between different applications in a matter of minutes, making the Empyrean a real multipurpose diffractometer.
Good laboratory practice
Empyrean with its alignment-free PreFIX modules and measurement and analysis automation possibilities supports anyone who has good laboratory practice (GLP) in mind. In addition, every aspect of the Empyrean package, from the hardware to dedicated analysis solutions, comes with extensive tutorials for novice users yet offers access to all functions for experts.
Customized solutions for X-ray diffraction
The Empyrean is a true multi-purpose instrument, designed to support a wide range of applications. Yet, in the market place we often meet scientists and analysts working with our equipment who would like to extend the possibilities even further, according to their own ideas for their own research. At Malvern Panalytical, we like to support our users in their materials research. We bring them the right solution for complex analytical problems or cost-effective production processes. If you have concepts for new sample holders and stages, optical modules or analytical techniques, discuss your requirements with your local Malvern Panalytical sales representative or submit your request if you need a dedicated solution for your diffraction research. Together we can work on advanced solutions for new requirements, keeping pace with the latest developments in the world of science and research.
Connected world
Smart Manager
Unleash the potential of your data
Until now, instrument data has too often been stuck in manual records, spreadsheets or site-specific servers. By connecting your Empyrean to our Smart Manager and continually analyzing instrument data in the cloud, you can unleash its full potential. This is just one of our digital solutions that are part of Malvern Panalytical's Smart Manager.
Key applications
Academia
Get the best data for your publications with Empyrean; train and inspire your students. Acquisition of comprehensive information about a material is the key for successful research. Empyrean will give you the highest data quality, letting you see the finest details of your precious samples by performing non-destructive, cutting-edge characterization studies.
Energy storage/ batteries
Get a better understanding of your battery materials. Analysis of battery material using X-ray diffraction provides component phase purity and the crystallite size of anode and cathode compounds. Empyrean equipped with the GaliPIX3D detector also allows in situ and in operando measurements of long-lasting cells using hard X-radiation.
Pharmaceuticals
Accomplish advanced characterization of your pharmaceuticals. X-ray powder diffraction, a rapid non-destructive analytical technique, is widely applied in drug discovery, formulation, stability testing and final product quality control. The proven and comprehensive method is available with 21 CFR Part 11 Audit Trail support. Empyrean can also perform in situ non- ambient analysis without manual intervention and high-throughput measurements on well-plates.
Specialty chemicals
Assess crystal structure or structure-property relationship in crystalline and semi-crystalline compounds. Specialty chemicals, also referred to as effect or performance chemicals, are often custom-manufactured materials with unique properties or performance effects to materials or formulation. Empyrean can be used for a detailed phase identification and understanding of these valuable compounds.
Forensics
Reveal the smallest traces of evidence. The use of non-destructive analytical instrumentation plays a key role in today’s forensic laboratories where full chain of custody and data control is desired across all stages of the process. Empyrean can provide information that is vital in criminal investigations and forensic science.
Metals
Determine retained austenite, stress and texture during metal production. Process control and quality control in the metal industry - whether it concerns primary metals or special products - need rapid and accurate chemical analysis as well as microstructural characterization of metals and alloys. Empyrean can take care of these needs.
Nanomaterials
Reveal dimensions and structures in all types of nanomaterials. X-ray scattering and diffraction are powerful and versatile nanometrology tools for the determination of nanoscale dimensions, shapes and structures, as well as the analysis of crystalline phases and local atomic structures. Empyrean delivers most accurate scattering data.
Thin film metrology
Get access to critical parameters of thin films ranging from ultra-thin single layers to complex multilayer stacks. X-ray diffraction and X-ray reflectivity can provide non-destructive, reliable and accurate data for the characterization of thin films. Empyrean enables the determination of ultra-fast reciprocal space maps, X-ray reflectivity and rocking curve analysis.
Specification
| X-ray generation | ||
|---|---|---|
| X-ray generator | 4 kW (max 60 kV, max 100 mA) | |
| Line/point focus switch | Easy and quick, without tooling | |
| Goniometer | ||
| Maximum usable range (depending on accessories) | -111 < 2θ < 168° | |
| Smallest addressable increment | 0.0001° | |
| Angular reproducibility | < 0.0002° | |
| 2θ linearity over whole range | Equal or better than ± 0.01° | |
| Maximum angular speed | 15 deg/s | |
| Angular resolution/td> | 0.026° FWHM on LaB₆ | |
| Sample stages | ||
| Ambient sample stages |
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| Non-ambient sample stages |
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| Detectors | ||
| Point detectors | Proportional counter (20 x 24 mm)
Scintillation detector (30 mm Ø) |
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| Strip detectors | PIXcel1D, 256 strips of 55 μm ‘all live’, compatible with Cr to Cu radiation | |
| Area detectors | PIXcel3D, 256 x 256 pixels of 55 μm, compatible with Cr to Cu radiation
GaliPIX3D, 501 x 465 pixels of 60 μm, compatible with Co to Ag radiation (with 100% efficiency) |
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| Cabinet | ||
| Exterior dimensions | 1400 (w) × 1162 (d) × 1947 (h) mm.
The instrument is on wheels. It can pass a 989 mm door opening. For transportation the minimum achievable instrument width is 867 mm. |
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| Weight | 1150 kg | |
| Accessibility of interior area | 1360 (w) × 1100 (h) mm, allowing access to the experimental area by at least four people simultaneously (ideal for teaching) | |
| Radiation level | Radiation level less than 1 microSievert per hour, measured at 10 cm distance, determined with a Mo source @ 60 kV, 50 mA. No power restrictions with all anode types | |
| Cooling water supply | 4 - 6 liters/min, pressure up to 8 bar, temperature 15 to 35 °C > dew point | |
| Compressed air supply | House line, compressor or air bottle; 2-5 bar (0.2 - 0.5 MPa) | |
| Power supply | Single phase 210 – 230 V (with ± 10% grid variations); 50/60 Hz | |
| Maximum power consumption* | 4.6 kVA | |
* without controllers for optional equipment
Accessories
Detectors
Software
X-ray diffraction software
Our XRD software packages are designed to extract every bit of information from your material.
X-ray tubes
Empyrean Tube
The Empyrean Tube is optimized for Malvern Panalytical's Empyrean diffractometers.
Non-ambient chambers
Non-ambient chambers
We offer a wide range of non-ambient solutions placing ‘in situ’ in front of nearly every application supported on our XRD instruments.
Support
Services
Solutions to maximize the return on your investment
To assure that your instrument remains in top condition and performs on the highest level, Malvern Panalytical offers a wide range of services. Our expertise and support services assure an optimal functioning of your instrument.
Support
Service for a lifetime
- Phone and remote support
- Preventive maintenance and checkups
- Flexible Customer Care Agreements
- Performance certificates
- Hardware and software upgrades
- Local and global support
Expertise
Adding value to your processes
- Sample preparation development/optimization
- Analytical methodologies
- Turnkey solutions for XRD
- Operations via IQ/OQ/PQ, quality assurance (GLP, ISO17025) or round robins/inter laboratory studies
- Consultancy services
Training and education
- Training on-site or at our competence centers
- Broad range of basic and advanced courses on products, applications and software
